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Content:
Chapter 1 Molecular and digital constitution of the amide crew (pages 1–72): M. B. Robin, F. A. Bovey and Harold Basch
Chapter 2 Synthesis of amides (pages 73–185): A. L. J. Beckwith
Chapter three Acid?base and complexing homes of amides (pages 187–243): R. B. Homer and C. D. Johnson
Chapter four Rearrangement and removing of the amido team (pages 245–288): Joseph F. Bieron and Frank J. Dinan
Chapter five Photochemistry of the amido workforce (pages 289–308): Ionel Rosenthal
Chapter 6 Radiation chemistry of amides (pages 309–334): Owen H. Wheeler
Chapter 7 Chemistry of imidic compounds (pages 335–381): Owen H. Wheeler and Oscar Rosado
Chapter eight The chemistry of thioamides (pages 383–475): W. Walter and J. Voss
Chapter nine The chemistry of the thiohydrazide crew (pages 477–514): W. Walter and okay. J. Reubke
Chapter 10 The chemistry of hydrazides (pages 515–600): Hans Paulsen and Dieter Stoye
Chapter eleven organic formation and reactions of the amido workforce (pages 601–684): J. E. Reimann and R. U. Byerrum
Chapter 12 Directing and activating results of the amido crew (pages 685–729): J. A. Shafer
Chapter thirteen Reactions of the carboxamide team (pages 731–857): Brian G. Challis and Judith A. Challis

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Sample text

Ncuman and Younge6 have shown that in the series of N,hTdimethylformamides in which the carbonyl oxygen is replaced by S, NH, and NHZ, the barrier height increases with l3C--IH coupling (23) at the formyl proton. The correlation is not impressive, however, as is small. the change in Ji3C--'EI The actual isolation of pure crystalline isomers of amides is reported by Siddall 93, who obtained two isomers of 23 and studied the ratcs of their interconversion in sym-tetrachlorocthane solution. The M.

Of course, thc use of a large cTo-basis set (compared to STO'S) means that one has that-many-times-more to the fourth power number of intcgrals to compute. But, multicentre integrals over GTO'S are evaluated using simple analytic formulas which are casily coded in simple FORTRAN language without recourse to complex numerical integration techniques, numcrous difficultly convergent expansions, or sophisticated programming structure. Thus the spced with which GTO integrals can bc computed more than compensates for the handicap of the largcr basis and the resultant need to computc the grcatcr number of integrals.

T,, and ~ o u p l i n g ~ ~This - ~ ~requires . thc use of a high-speed digital coniputer to generate thc theoretical spectra, which may then be compared visually with the experimental spectra. r. r. arc availablc and have been applied to amides. O n e procedure is to extend the rathcr limited temperature range available for such studies by employing ‘wiggle decay’ measurements of the narrow line widths well abovc and lxlow coalescence, where direct measurements are inaccurate. This is in effect a more precise mcasurcment of T,.

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