Download Coal and Coal-Related Compounds, Volume 150: Structures, by Toshiaki Kabe, Atsushi Ishihara, Eika Weihua Qian, I. Putu PDF

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By Toshiaki Kabe, Atsushi Ishihara, Eika Weihua Qian, I. Putu Sutrisna, Yaeko Kabe

Coal is extra ample than petroleum and average gasoline. additional, coal isn't really localized yet can be utilized by way of many extra nations than petroleum. for that reason, if we will be able to identify coal usage know-how, coal will lead to a good contribution to human existence and society. nonetheless, scarcity of petroleum and typical gasoline are expected within the moment 1/2 the twenty first century. To compensate, using coal is anticipated to steadily elevate in the course of the twenty first century. sooner or later, the advance of the coal usage expertise turns into increasingly more vital to insure the provision of liquid fuels for transportation and carbon assets for the manufacture of chemical compounds and plastic materials.

In order to boost such applied sciences, the elucidation of the constitution of coal is a basic zone of analysis. additional, extra effective coal usage know-how has to be validated to fulfill environmental laws. one of many key applied sciences for this goal is catalysis. This quantity offers aspect of the fundamental and useful elements of the technological know-how and know-how of coal usage with and with out catalysts. the particular constitution of coal, the chemistry integrated within the reactivity of coal, the tips on how to elucidate the constitution of coal and re-action mechanisms of coal conversion, an important catalyst for changing coal to liquid and gasoline, the function of the catalysts in coal conversion, the issues within the technique engineering, and the way to satisfy environmental rules are mentioned intimately. the hot growth in stories at the constitution and reactivity of coal revamped the final century is summarized and reviewed with emphasis on either primary and utilized facets of the technological know-how and expertise for coal processing within the presence and shortage of catalysts.

* This publication highlights the problems confronted in attempting to realize extra effective coal usage technology.
* offers specific dialogue on the way to meet environmental rules and laws.
* Fills the distance among either the clinical and useful aspects of coal usage with and with out catalysts.

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Additional resources for Coal and Coal-Related Compounds, Volume 150: Structures, Reactivity and Catalytic Reactions

Example text

Thus, it is likely that for the reaction, the rate-limiting step is not the speed of the exchange reaction between water and coal but the diffusion of water into the coal. That is, temperature in fact affects the diffusion rate of the water into coal. When the hydrogen exchange with tritiated water was carried out using other coals, 40 1 Methods of Classification and Characterization of Coal 10 = 4 2 9 100~ II 50 ~ 0 , 0 I 1 , I 2 , t 3 , ~ 4 , ~ , t , ~ , i 5 6 7 8 Reaction time (h) , i , 9 I , 10 I , 1~2 , 11 13 Fig.

One reaction procedure is as follows. One gram of coal and 1 g tritiated water (initial radioactivity 106 dpm) were added into a 25-ml Pyrex glass reactor. After the mixture was degassed in vacuum via three freeze-pump-thaw cycles, the reactor was immersed into an oil bath and the reaction mixture was stirred with a magnetic stirrer. The reaction temperatures were 50 ~ and 100 ~ and the reaction times were 1-24 h. After the reaction, the reaction mixture was separated into tritiated water and coal with a vacuum line ( ~ 10 -4 T o r r ) .

Every tritiated water sample (ca. 4 g) was dissolved into 14 ml of a scintillator solvent (Monophase S) and the radioactivity of the obtained solution was measured with a liquid scintillation counter. After drying in vacuum at 50 ~ or 100 ~ for 7 h, tritiated coal was oxidized by an automatic sample combustion system into tritiated water to measure its radioactivity. The reactions of model compounds with tritiated water were performed in a similar way. After the reaction, the tritiated model compounds were isolated by filtration or by distillation.

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