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By Allan S. Myerson, Ken Toykura

content material: Crystallization examine within the Nineteen Nineties : an outline / Allan S. Myerson --
critical equation research of homogeneous nucleation / Günther H. Peters, John Eggebrecht, and Maurice A. Larson --
Solubilities in multicomponent platforms / Jaroslav Nývlt and Jiří Stávek --
Hardness of salts utilized in commercial crystallization / J. Ulrich and M. Kruse --
Calculation of crystal behavior and solvent-accessible components of sucrose and adipic acid crystals / Allan S. Myerson and Michael Saska --
Sucrose crystal development : conception, test, and commercial purposes / D. Aquilano, M. Rubbo, G. Mantovani, G. Vaccari, and G. Sgualdino --
elements affecting the purity of L-isoleucine recovered by way of batch crystallization / Ronald C. Zumstein, Timothy Gambrel, and Ronald W. Rousseau --
Light-scattering measurements to estimate kinetic parameters of crystallization / W.R. Witkowski, S.M. Miller, and J.B. Rawlings --
Double draw-off crystallizer : significant participant within the acid rain video game? / Alan D. Randolph, S. Mukhopadhyay, B.C. Sutradhar, and Ross Kendall --
Hydrocyclones for measurement type in non-stop crystallizers / Johan Jager, Sjoerd de Wolf, Herman J.M. Kramer, and Esso J. de Jong --
Derivation of kingdom house types of crystallizers / Sjoerd de Wolf, Johan Jager, B. Visser, Herman J.M. Kramer, and O.H. Bosgra --
Simulation of the dynamic habit of constant crystallizers / Herman J.M. Kramer, Sjoerd de Wolf, and Johan Jager --
Crystal measurement distribution and features linked to a continual crystallizer / Yoshio Harano, Shogo Sudo, and Yoshio Aoyama --
Kinetics of the ethanolic crystallization of fructose / M.R. Johns, R.A. pass judgement on, and E.T. White --
advancements in controlling directed crystallization and sweating / J. Ulrich and Y. Özoguz --
In situ commentary of p-xylene crystal progress via controlling strain / Masato Moritoki and Nobuhiko Nishiguchi --
Solute move in sector refining of eutectic-forming combinations / George C. Yeh --
Purity lessen of L-threonine crystals in optical solution by way of batch preferential crystallization / Masakuni Matsuoka, Hirokazu Hasegawa, and Koichi Ohori --
Semi-batch cooling crystallization of quizalofop-ethyl with polymorphism / Akihiro Shiroishi, Isao Hashiba, Ryo Kokubo, Kazuo Miyake, and Yuji Kawamura --
progress expense of S-carboxymethyl-D-cysteine and its optical solution / M. Yokota, T. Oguchi, okay. Arai, Ken Toyokura, C. Inoue, and H. Naijyo --
commentary of high-pressure crystallization of benzene from benzene-cyclohexane combination / Hideo Narahara, Kenji Yamada, Ken Toyokura, Masato Moritoki, and Nobuhiko Nishiguchi --
Crystallization of gypsum from phosphoric acid ideas / E.T. White and S. Mukhopadhyay --
Crystallization of ice from aqueous ideas in suspension crystallizers / Yuping Shi, Baomin Liang, and Richard W. Hartel --
Kinetics of secondary nucleation of alumina trihydrate in a batch crystallizer / H.M. Ang and P.I.W. Loh --
Reactive crystallization of magnesium hydroxide / Hideki Tsuge and Hitoshi Matsuo --
Fluidized-bed technique for phosphate elimination through calcium phosphate crystallization / Izumi Hirasawa and Yasunori Toya --
Freeze focus of aqueous options / Tasoula C. Kyprianidou-Leodidou and Gregory D. Botsaris --
form issue of a magnesium sulfate crystal starting to be in its aqueous resolution / Yoji Taguchi, Takashi Matsumura, Masayuki Satoh, and Tetsuya Ohsaki --
non-stop crystallization of calcium sulfate stages from phosphoric acid recommendations / G.J. Witkamp and G.M. van Rosmalen --
Acceleration phenomenon on solidification of CaCl₂·6H₂O with a nucleation agent / Yasuyuki Watanabe, Tomonari Saito, and Tasuku Nakai.

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The photos of indentations by the Vickers pyramid i n a sodium chlorate c r y s t a l are presented i n Figure 2 and give an idea of r e s u l t i n g cracks and l i f t - o f f s . 6 N). In the case of potassium n i t r a t e the Vickers hardness indentat i o n s have not a quadratic shape. This i s due t o a d i r e c t i o n dependent hardness i n the c r y s t a l l a t t i c e of t h i s material. ch004 46 CRYSTALLIZATION AS A SEPARATIONS PROCESS 4. ch004 t i c e . The force-dependency o f the Vickers hardness isshown i n the p l o t i n Figure 3.

The force-dependency o f the Vickers hardness isshown i n the p l o t i n Figure 3. In the diagram there are two curves of the Vickers hardness r e s u l t i n g always from the same indentation image. The hardness values d i f f e r by a f a c t o r of two. The one curve r e s u l t s from the data o f the longer and the other from the shorter diagonal o f each intendation. This d i r e c t i o n dependency was so f a r only observed for the case of potassium n i t r a t e . Also the e f f e c t of impurities i n a c r y s t a l on the Vickers hardness was analysed.

16. 17. 18. 19. 20. 21. Tai, C. ; McCabe, W. L . ; Rousseau, R. W. AIChE Journal 1975, 21, 351. ; Ulrich, J . Verfahrenstechnik 1980, 14, 815. Ulrich, J . D. Thesis, RWTH Aachen, Aachen FRG, 1981. ; Ulrich, J . In Industrial Crystallization 81; Jancic, S. ; de Jong, E. ; Elsevier: Amsterdam, 1981, p 313. Heffels, S. K. D. Thesis, TH Delft, Delft NL, 1986. Pohlisch, R. J . D. Thesis, TU München, München FRG, 1987. Offermann, H. ; Elsevier: Amsterdam, 1989, p 121. ; Pohlisch, J . Chem. Eng. Tech.

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