By Richard W. Bukowski
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The XCCo3(CO)9 to (OC)9Co3CCO+ conversion is an intriguing one which necessarily involves a migration of CO from cobalt to the apical carbon atom, but its mechanism is not yet fully understood. : BrCCo 3 (CO) 9 MeOH reflUX ' under CO BrCCo 3 (CO) 9 Et2N ► ( O C ) 9 C o 3 C C 0 2 M e + HBr (128) ► ( O C ) 9 C o 3 C C ( 0 ) N E t 2 + HBr (129) (86%) ";rapidat room temperature (79%) Triethylamine is effective in inducing such reactions (Seyferth and Nivert, 1976): BrCCo3(CO)9 M e H > 25 ° 24 hr ° .
And Kettle, S. F. A. (1971). Chem. Commun, p. 282. Bamford, C. , Eastmond, C. , and Maltman, W. R. (1964). Trans. Faraday Soc. 60, 1432. Barlex, D. M, Kemmitt, R. D. W, and Littlecott, G. W. (1969). Chem. Commun, p. 613. Barlex, D. , Kemmitt, R. D. W, and Littlecott, G. W. (1972). J. Organomet. Chem. 43, 225. Bennett, M. , Robertson, G. B, Whimp, P. O, and Yoshida, Y. (1971). J. Am. Chem. Soc. 93, 3797. Bennett, M. , Johnson, R. , Robertson, G. , Turney, T. W, and Whimp, P. O. (1972). J. Am. Chem.