By Ronald S. Bauer (Eds.)
Content material: The photoinitiated cationic polymerization of epoxy resins / J.V. Crivello and J.H.W. Lam -- Photosensitized epoxides as a foundation for light-curable coatings / William R. Watt -- Quaternary phosphonium compound latent accelerators for anhydride-cured epoxy resins / James D.B. Smith -- improvement of epoxy resin-based binders for electrodeposition coatings with excessive corrosion resistance / W. Raudenbusch -- Water-borne coatings ready from excessive molecular weight epoxy resins / Edward G. Bozzi and Camilla Y. Zendig -- Aqueous epoxy resins for electric strengthened plastics / Terry L. Anderson, James H. Melloan, Kathleen L. Powell, Roland R. McClain, J. Brandon Simons, Robin L. Conway, and David A. Shimp -- Epoxide similar weight selection through carbon-13 nuclear magnetic resonance / W.B. Moniz and C.F. Poranski, Jr. -- An instrumental strategy for measuring the sterilization resistance (blushing) of can coatings / W. Raudenbusch, H.C.J. Venselaar, and D.M. Paul -- Phenalkamines, a brand new classification of epoxy curing brokers / Robert A. Gardiner and Anthony P. Manzara -- The impact of alkyl substituents at the homes of cured hydantoin epoxy resins / E.H. Catsiff, R.E. Coulehan, J.F. Diprima, D.A. Gordon, and R. Seltzer -- impression of cross-link density distribution at the engineering habit of epoxies / S.C. Misra, J.A. Manson, and L.H. Sperling -- community morphology and the mechanical habit of epoxies / S.C. Misra, J.A. Manson, and L.H. Sperling -- Creep habit of amine-cured epoxy networks : impact of stoichiometry / S.L. Kim, J.A. Manson, and S.C. Misra -- Self-cross-linkable polyepoxides / Yoshio Tanaka -- a few reviews at the education of glycidyl 2-ethylhexanoate / D.A. Cornforth, B.G. Cowburn, K.M. Smith, C.W. Stephens, and C.G. Tilley -- Reactions in a standard epoxy-aliphatic diamine approach / John J. King and James P. Bell -- Epoxy resins containing a selected vulnerability / James R. Griffith
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Additional resources for Epoxy Resin Chemistry
While capable o f r a p i d c u r e , the c o a t i n g must be s u f f i c i e n t l y s t a b l e t h a t i t does not undergo a p p r e c i a b l e change i n the period between a d d i t i o n o f the p h o t o i n i t i a t o r and a p p l i c a t i o n to the object being coated. T h i s i n t e r v a l may be a few hours ( o n - s i t e mixing) or several months, as would be the case w i t h coatings prepared at a c e n t r a l l o c a t i o n and stored f o r extended periods p r i o r to d i s t r i b u t i o n and use.
T r i p h e n y l s u l f o n i u m hexafluorophosphate can be prepared from diphenyliodonium hexafluorophosphate by heating w i t h phenyl s u l f i d e , as described by Knapczyk and McEwen ( 5 9 ) , or by r e a c t i o n o f phenyl magnesium bromide w i t h d i p h e n y l s u l f o x i d e followed by r e a c t i o n w i t h hexafluorophosphoric a c i d according to the procedure o f W i l d i , T a y l o r and P o t r a t z (60). Comparison o f P h o t o i n i t i a t o r s Two p r o p e r t i e s of fundamental importance to the successful f u n c t i o n i n g o f a p h o t o i n i t i a t o r f o r l i g h t - c u r a b l e coatings are cure r a t e and storage s t a b i l i t y o f the p h o t o s e n s i t i z e d formulations.
The second s t e p , w h i l e independent o f UV r a d i a t i o n , i s influenced by heat. Continuous exposure to a mercury arc to determine t a c k free time can i n f l u e n c e the course o f the p o l y m e r i z a t i o n because of an increase i n temperature of c o a t i n g and s u b s t r a t e caused by the intense heat o f the mercury a r c . To avoid t h i s c o m p l i c a t i o n and to maintain c o n t r o l o f the temperature o f the c o a t i n g during c u r e , exposure to the mercury arc was g e n e r a l l y l i m i t e d to two seconds.