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By Howard Alper (Eds.)

Transition steel Organometallics in natural Synthesis. quantity II

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F. C , Mays, M. J , and Howell, J. A. S. (1976). Inorg. Chim. Acta 20, L41. , and Sappa, E. (1967). J. Organomet. Chem. 8, 149. Chatt, J , and Duncanson, L. A. (1953). J. Chem. Soc. p. 2939. Chisholm, M. , and Clark, H. C. (1971). Inorg. Chem. 10, 2557. Chisholm, M. , and Clark, H. C. (1972). J. Am. Chem. Soc. 94, 1532. Chisholm, M. , and Clark, H. C. (1973). Ace. Chem. Res. 6, 202. Chisholm, M. H , Clark, H. C , Manzer, L. E , and Stothers, J. B. (1972). J. Am. Chem. Soc. 94, 5087. Chukhadzhyan, G.

The XCCo3(CO)9 to (OC)9Co3CCO+ conversion is an intriguing one which necessarily involves a migration of CO from cobalt to the apical carbon atom, but its mechanism is not yet fully understood. : BrCCo 3 (CO) 9 MeOH reflUX ' under CO BrCCo 3 (CO) 9 Et2N ► ( O C ) 9 C o 3 C C 0 2 M e + HBr (128) ► ( O C ) 9 C o 3 C C ( 0 ) N E t 2 + HBr (129) (86%) ";rapidat room temperature (79%) Triethylamine is effective in inducing such reactions (Seyferth and Nivert, 1976): BrCCo3(CO)9 M e H > 25 ° 24 hr ° .

And Kettle, S. F. A. (1971). Chem. Commun, p. 282. Bamford, C. , Eastmond, C. , and Maltman, W. R. (1964). Trans. Faraday Soc. 60, 1432. Barlex, D. M, Kemmitt, R. D. W, and Littlecott, G. W. (1969). Chem. Commun, p. 613. Barlex, D. , Kemmitt, R. D. W, and Littlecott, G. W. (1972). J. Organomet. Chem. 43, 225. Bennett, M. , Robertson, G. B, Whimp, P. O, and Yoshida, Y. (1971). J. Am. Chem. Soc. 93, 3797. Bennett, M. , Johnson, R. , Robertson, G. , Turney, T. W, and Whimp, P. O. (1972). J. Am. Chem.

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