By Howard Alper (Eds.)
Transition steel Organometallics in natural Synthesis. quantity II
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Additional info for Transition Metal Organometallics in Organic Synthesis
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The XCCo3(CO)9 to (OC)9Co3CCO+ conversion is an intriguing one which necessarily involves a migration of CO from cobalt to the apical carbon atom, but its mechanism is not yet fully understood. : BrCCo 3 (CO) 9 MeOH reflUX ' under CO BrCCo 3 (CO) 9 Et2N ► ( O C ) 9 C o 3 C C 0 2 M e + HBr (128) ► ( O C ) 9 C o 3 C C ( 0 ) N E t 2 + HBr (129) (86%) ";rapidat room temperature (79%) Triethylamine is effective in inducing such reactions (Seyferth and Nivert, 1976): BrCCo3(CO)9 M e H > 25 ° 24 hr ° .
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